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API MPMS CH 10.8, 3rd Edition: Standard Test Method for Sediment in Crude Oil by Membrane Filtration

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ISO 1690:1976

ISO 1690:1976 Sodium and potassium silicates for industrial use – Determination of silica content – Gravimetric method by insolubilization

CDN $86.00

SKU: ff56777c54d5 Category:

Description

The procedure is based on evaporation to dryness of a test portion previously acidified with hydrochloric acid. Dissolution of the soluble salts, filtration and washing of the insoluble matter. Second evaporation of the filtrate and washings under the same conditions, further dissolution of the soluble salts, filtration and washing. Calcination and weighing of the two lots of insoluble matter simultaneously. Volatilization of silica by heating with hydrofluoric and sulphuric acids and weighing of the residue after calcination. The*difference in mass represents the silica present in the test portion.

Edition

1

Published Date

1976-02-01

Status

PUBLISHED

Pages

3

Language Detail Icon

English

Format Secure Icon

Secure PDF

Abstract

The procedure is based on evaporation to dryness of a test portion previously acidified with hydrochloric acid. Dissolution of the soluble salts, filtration and washing of the insoluble matter. Second evaporation of the filtrate and washings under the same conditions, further dissolution of the soluble salts, filtration and washing. Calcination and weighing of the two lots of insoluble matter simultaneously. Volatilization of silica by heating with hydrofluoric and sulphuric acids and weighing of the residue after calcination. The*difference in mass represents the silica present in the test portion.

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