ISO 5993:1979
ISO 5993:1979 Sodium hydroxide for industrial use – Determination of mercury content – Flameless atomic absorption spectrometric method
CDN $76.00
Description
Covers a method applicable to liquid or solid products having mercury contents greater than 0,02 mg/kg. The principle of determination is based on oxidation of the mercury contained in a test portion to mercury(II) ions by potassium permanganate in the presence of sulphuric acid, reduction of the excess oxidant by hydroxylammonium chloride, reduction of the mercury(II) ions to mercury by tin(II) chloride, entrainment of the mercury in air or nitrogen, passage of the gaseous mixture through a measuring cell, and measurement of the absorption at a wavelength of 253,7 nm.
Edition
1
Published Date
1979-09-01
Status
PUBLISHED
Pages
6
Language
English
Format
Secure PDF
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Abstract
Covers a method applicable to liquid or solid products having mercury contents greater than 0,02 mg/kg. The principle of determination is based on oxidation of the mercury contained in a test portion to mercury(II) ions by potassium permanganate in the presence of sulphuric acid, reduction of the excess oxidant by hydroxylammonium chloride, reduction of the mercury(II) ions to mercury by tin(II) chloride, entrainment of the mercury in air or nitrogen, passage of the gaseous mixture through a measuring cell, and measurement of the absorption at a wavelength of 253,7 nm.
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