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API STD 521: Guide for Pressure-relieving and Depressuring Systems – Edition 6

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ISO 4327:1979

ISO 4327:1979 Non-ionic surface active agents – Polyalkoxylated derivatives – Determination of hydroxyl value – Phthalic anhydride method

CDN $124.00

SKU: 1ca06225b97d Category:

Description

The hydroxyl groups are esterified by phthalic anhydride in pyridine solution. The excess of phthalic anhydride is hydrolyzed with water containing in the sodium hydroxide solution used for the neutralization. The acidity which appears during the esterification and of the phthalic acid formed during the hydrolysis is neutralized by sodium hydroxide solution in the presence of phenolphthalein as indicator. The hydroxyl value is calculated from the difference between the volumes of sodium hydroxide solution used for the titration of the blank and of the test solution.

Edition

1

Published Date

1979-12-01

Status

PUBLISHED

Pages

8

Language Detail Icon

English

Format Secure Icon

Secure PDF

Abstract

The hydroxyl groups are esterified by phthalic anhydride in pyridine solution. The excess of phthalic anhydride is hydrolyzed with water containing in the sodium hydroxide solution used for the neutralization. The acidity which appears during the esterification and of the phthalic acid formed during the hydrolysis is neutralized by sodium hydroxide solution in the presence of phenolphthalein as indicator. The hydroxyl value is calculated from the difference between the volumes of sodium hydroxide solution used for the titration of the blank and of the test solution.

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