ISO 2828:1973
ISO 2828:1973 Aluminium oxide primarily used for the production of aluminium – Determination of fluorine content – Alizarin complexone and lanthanum chloride spectrophotometric method
CDN $82.00
Description
Applicable to products having F contents of more than 0.003 % (m/m). Dissolution of a test portion by attack by sulphuric acid under pressure. Separation of the fluorine by distillation at a temperature of (150 1) °C by sulphuric acid. The distillation is carried out by the method described in ISO 1693. Formation of a blue coloured complex between fluorine and alizarin complexone/lanthanum chloride reagent at a pH between 4.5 and 4.6. Addition of acetone to increase the stability and sensitivity of the fluorine complex. Spectrophotometric measurement of the complex at a wavelength of about 620 nm. Has also been approved by the IUPAC.
Edition
1
Published Date
1973-12-01
Status
PUBLISHED
Pages
3
Language
English
Format
Secure PDF
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Abstract
Applicable to products having F contents of more than 0.003 % (m/m). Dissolution of a test portion by attack by sulphuric acid under pressure. Separation of the fluorine by distillation at a temperature of (150 1) °C by sulphuric acid. The distillation is carried out by the method described in ISO 1693. Formation of a blue coloured complex between fluorine and alizarin complexone/lanthanum chloride reagent at a pH between 4.5 and 4.6. Addition of acetone to increase the stability and sensitivity of the fluorine complex. Spectrophotometric measurement of the complex at a wavelength of about 620 nm. Has also been approved by the IUPAC.
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