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B51-14 (R2019) – Boiler, pressure vessel, and pressure piping code

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ISO 6228:1980

ISO 6228:1980 Chemical products for industrial use – General method for determination of traces of sulphur compounds, as sulphate, by reduction and titrimetry

CDN $129.00

SKU: 07a3acc09c3f Category:

Description

Describes a method based on prior conversion of the sulphur compounds in a test portion to sulphate, if required, and reduction of the sulphate ions ti hydrogen sulphide by a mixture of hydriodic and phosphinic acids in the presence of hydrochloric acid. The hydrogen sulphide is entrained in a current of nitrogen and absorbed in a solution of sodium hydroxide in aqueous acetone, followed by titration of the sulphide ions with standard volumetric mercury(II) acetate or nitrate solution in the presence of 1,5-diphenyl-3-thiocarbazone (dithiozone) as indicator.

Edition

1

Published Date

1980-11-01

Status

PUBLISHED

Pages

7

Language Detail Icon

English

Format Secure Icon

Secure PDF

Abstract

Describes a method based on prior conversion of the sulphur compounds in a test portion to sulphate, if required, and reduction of the sulphate ions ti hydrogen sulphide by a mixture of hydriodic and phosphinic acids in the presence of hydrochloric acid. The hydrogen sulphide is entrained in a current of nitrogen and absorbed in a solution of sodium hydroxide in aqueous acetone, followed by titration of the sulphide ions with standard volumetric mercury(II) acetate or nitrate solution in the presence of 1,5-diphenyl-3-thiocarbazone (dithiozone) as indicator.

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